THE COLLIERY GUARDIAN AN® JOURNAL OF THE COAL AND IRON TRADES. Vol. CXVI. FRIDAY, AUGUST 2, 1918. No. 3005. Cementation Process Applied to Mining.* By A. H. KRYNAUW. During recent years experience has proved that cement can be introduced, under pressure, into the minutest fissures and cracks in rock strata, as well as cracks and interstices in masonry and concrete constructions, and made to set there. This practice of introducing cement grout under pressure has evolved to that known to-day as the Francis cementation process. An essential condition in the introduction of cement into fissures and cracks is that the injection should be done under a considerable pres- sure, the object being, firstly, to overcome the contra pressure of water present in the fissure; secondly, for the purpose of forcing the cement as far as pos- sible into the minute cracks; and, thirdly, for the purpose of squeezing out the superfluous water from the cavity which is being filled with cement pulp, and thus leave the cement in a condition most suit- able for its rapid and efficient setting. Conditions of Setting. Cement milk, when allowed to set ordinarily under water, does so only very slowly and reluctantly, but when the same milk is subjected to pressure, such as produced by a specially constructed cementation pump, the cement sets hard within 24 hours. The setting of cement is chiefly due to the inter-crystallisa- tion of hydrated calcic silicate and hydrated calcic aluminate, just the necessary amount of water being taken up to complete the crystallisation; the crystals grow together and form a hard mass. Now, when a superabundance of water is present, such as in the mixture used in cementation work, these crystals ordinarily seem reluctant to inter-crystallise; conse- quently the setting of the cement is very slow and incomplete. The condition most suitable for hard setting in the shortest time, when the cement is pumped under pressure into fissures, etc., appears to be somewhat as follows: First of all, the constricted exits of the fissures are choked with cement pulp, which forms a filter bed on which successive layers of cement are deposited, the surplus water being squeezed out through the cement filter already formed in the peripheral areas of the fissure or cavity. As more cement solution is injected the pressure gradually rises, and goes on rising, owing to the. fact of the water having to be squeezed through an increasing thickness of cement filter. The successive layers of cement eventually fill the fissure or cavity completely, leaving the cement in a condition suitable for com- plete and good setting. Pressures of 1,000 lb. to 4,000 lb. ‘ per sq. in. are used, and for this purpose a specially designed pump is employed, of the double ram hori- zontal type with a 12 in. stroke, the steam end having a diameter of 14 in., and the water end a plunger diameter of If in. to 3 in., depending on the final pressure likely to be required. As the wear on the valves is great, hardened steel balls are used. Application of the Cementation Process. In the following cases cementation has been success- fully applied : — 1. In greatly minimising water difficulties in shaft sinking or tunnelling through water-bearing strata, faults and dikes. 2. In sealing and rendering water-tight the concrete tubbing or lining often used in circular shafts. 3. In sealing open fissures through which water is flowing. 4. In damming back water leaking through broken ground, in the vicinity of faults and dikes. 5. In rendering underground dams water-tight. 6. In rectifying defective boreholes. 7. In rendering impervious the foundations of surface dams or making solid the rock and concrete foundations of engines, etc. Shaft Sinking. The process as applied to shaft sinking consists of a treatment of the strata, through which the shaft is to be sunk, with cement grout, which is injected into the fissures and cracks of the rock mass, thus sealing them and rendering the ground practically free of water. The method of carrying out the work is as follows: A system of drill holes is put down on the periphery of the shaft, and through these holes a thin cement mixture is introduced, which finds its way into the cracks and crevices, rendering them impervious to water. There are two methods of carry- ing this out. In the Portier method the holes are put outside the perimeter of the shaft, and it is claimed that this has the advantage of permitting the sinking of the shaft simultaneously with the injection of the cement. This is a very strong point, in that it practi- cally overcomes the interruption and delay to the * From paper submitted to the monthly meeting of the Chemical, Metallurgical and Mining Society of South Africa on May 18. sinking of the shaft while conducting the process. On the other hand, the Portier system is attended by the following disadvantages: — (a) The possible deflection of the boreholes into the shaft, rendering them useless for the subsequent injection of cement. ■(b) The danger to sinkers, when applying great pressure in the boreholes, owing to the possi- bility of rupturing the sides of the shaft. (c) The boreholes may intercept several fissures, but the mouth of the hole being above the water level, it is not possible to tell which fissure is the chief water carrier, so that when injection takes place the tendency will be for the cement to take the course of least resistance into the larger fissures, while the smaller ones, though probably of considerable importance, are only sealed in the vicinity of the hole itself. In the Francis system the boreholes through which the cement is introduced are put down, within the limits of the shaft, arranged on the perimeter Fig. 1. f « n li i i l 11 H II ‘ II £ II * r ; U ii n at various distances apart, depending on the size of shaft and thickness of rock strata to be treated. The detailed method of procedure is indicated by the following description of the work being done at the Daggafontein and Brakpan mines : — Daggafontein Sinking. Daggafontein No. 2 Shaft is a seven-compartment rectangular shaft, 49 ft. long by 9 ft. wide, and was sunk from the surface to 175 ft. in dwyka conglomerate containing numerous cavities and fissures, giving a fair amount of water, but not of such quantity as to seriously hinder sinking. At a depth of 354 ft. the syenite dike of the far East Rand was encountered, and the shaft sunk in it to its present depth of 500 ft. At this stage the water dealt with amounted to 21,000 gallons per hour, and the management decided to put down a pilot borehole to ascertain the nature of the strata ahead. This hole intercepted the dolomite series at a depth of 12 ft. below the shaft bottom, and at a depth of 165 ft. a considerable amount of water was encountered. In view of the probability of large quantities of water being met with in the dolomites, shaft sinking was stopped, and the adop- tion of the Francis cementation process decided upon. From the data available the thickness of the dolomite formation was estimated at 200 ft., the direc- tion of the boreholes being set out accordingly, so as to permit of a single stage treatment for the full width of the strata. Unfortunately, the thickness of the dolomites proved to be considerably more than anticipated, being a total of 345 ft., which distance was considered too much for treatment in one stage. A distinct open parting exists at the contact of the syenite dike and underlying dolomite. This was clearly demonstrated, for when drilling through the dolomite contact the feed water was forced out of holes previously drilled. At a depth of 35 ft. the first feeder was met with containing sufficient water to cause a flow of 250 gallons per hour out of a 1| in. drill hole. A second and larger fissure was struck at a depth of about 130 ft., and as each hole intercepted water, cement grout was injected, the progress of the injection being observed by the rise in pressure indicated on a pressure gauge. When a pressure of 2,000 lb. per sq. in. was reached, pumping was stopped and the cement allowed to set. In all 55 tons of cement were used, and as the depth of the holes is about 180 ft., sinking can now be continued for that depth. Brakpan Sinking. Brakpan No. 3 Shaft is a 20 ft. diameter circular shaft, and from the surface to 162 ft. is sunk in dwyka conglomerate. At a depth of 170 ft. the syenite dike was met, and sinking was continued through this dike and for 6 ft. into the underlying dolomites. At this point a sudden inrush of water occurred which flooded the shaft to a depth of 80 ft. in a very short while, the suddenness of the inrush causing the death of a native. The method to be applied at this shaft will be similar to that employed at Daggafontein, except that in this case the shaft had in the first instance to be dewatered by pumping and baling, and when sufficiently dry a concrete plug about 5 ft. thick was placed on the shaft bottom, with a release pipe to take off the water while laying the concrete matt. After allowing the concrete time to set, holes will be put down and the treatment carried out in a manner similar to that already described. In this instance, however, the dolomite beds being only 140 ft. thick, one stage treatment will be sufficient. Even had this inrush of water occurred at a much greater depth with considerable pressure, and in such quantity that the shaft could not be conveniently dewatered, the concrete plug could be put at the shaft bottom with no great difficulty, advantage being taken of the water rising in the shaft to its natural head. Tunnelling. When required to drive a tunnel through a water zone, the method adopted is very similar to that just described for shafts, and the results obtained at the East Rand Proprietary Mines in this connection have been very satisfactory. Two different examples of this work were conducted, the first being a case where the water was unexpectedly struck in the 30 Level West Drive. In this instance a 12 ft. brick dam was built with certain pipes arranged through it to allow of the water escaping while building the dam and to permit of cementation being subsequently carried out. It should be noted that at the West Shaft, 1,500 ft. away from this point, a borehole had struck water of the same pressure, suggesting the same source of water as in this drive, and as proof of this when injecting at this dam some cement came out of the borehole in the West Shaft, clearly showing how well the cement at times will travel. ( Colloidal Injection. During cementation work at the Hatfield Main Colliery, it. was practically impossible to force the cement into the fissures in the old red sandstone forma- tion. The cement would not travel any distance, but set immediately in the vicinity of the boreholes. Mr. Francis hit upon the idea that the trouble was due to the fissures being all more or less filled with sand and dirt, the product of the sandstone, and that when forcing the cement into these fissures the sand would act as a filter bed and the cement would immediately pack into a mass. To overcome this, solutions of silicate of soda and sulphate of alumina were separately injected into the fissures. These chemicals react on each other and form in the fissures a gelatinous or colloidal substance, which being forced through carry away the sand, leaving the fissures open and clear to receive the cement. It also seems to line the walls of the fissure with a thin smooth layer of chemicals, and thus acts in the manner of a lubri- cant which nullifies the frictional resistance of the walls of the fissure. Sealing Ferro-Conorefe Shaft Lining. In shaft sinking, particdiarly circular shafts, a lining of ferro-concrete or bricks is generally adopted, and in this connection it frequently becomes desirable to dam back water behind the lining. As this water may be under a considerable pressure, the problem is no easy one unless a process such as the Frangois method is adopted. In this instance a number of weep pipes are built in with the lining, which allows the escape of the water while the lining is being con- structed, thus relieving the “ green wall ” of the water pressure. After allowing the lining sufficient time to set, the weep pipes are in turn connected to the cementation pump, and cement grout is injected behind the lining and into the fissures, thus sealing them up. Should the lining of the shaft not be of