1084 THE COLLIERY GUARDIAN. November 26, 1915. CURRENT SCIENCE Automatic Sampling of Coal. L. C. Bosler, in Power, describes an automatic coal sampling device, by which all of the coal received is sampled without the human element entering into the operation at all. Coal is received in boats, and is unloaded therefrom by two electrically-driven loco- motive cranes on the pier. The coal is dumped into cars, where it is weighed, and is then delivered to a conveyor, and carried to the crusher. The coal at this point is reduced to a size not greater than Sin. in diameter. It is then raised to a height equal to the elevation of the top of the coal bunkers, and is then conveyed to them. The sampling device is in this last- named conveyor. The hopper for catching the major sample is underneath. Beneath this is a rotary crusher and automatic sampler, which receives the coal from the hopper. This machine performs two separate and dis- tinct functions : it first grinds the major sample to any desired size, and then divides it into two parts, one of which is the final sample, it being drawn from the front spout, while the balance falls back into the bunker through the side spout. By operating the adjusting wheel on the grinder, any proportion desired can be obtained between the final and the major sample. Connor Spout fbr\ sampling ' coal Surplus '/spout Fig. 1.—Conveying and Sampling Machine. E H * Trough Fig. 2.—Gate-operating Mechanism. On a flight of the conveyor is fastened a plate A. With the movement of the conveyor to the left this plate engages with the roller B, and thereby raises the arm C. With this movement the arm D is also raised, as both are keyed to the shaft E. As the arm D rises, it pulls up the arm F, which, through the shaft G, is keyed to the arm H. At the end of this arm is fastened the rod J, which operates the gate. This gate is closed by the use of a counter-weight attached to the arm F. By the pull rod K, and yoke lever L, the arm C can be slid on the shaft E out of the path of the plate A, thereby cutting the apparatus out of service. It will be seen that there must be a fixed relation between the position of the flight and the opening of the gate. With the gate wide open when the flight reaches the near side of the hole, the maximum dis- charge will take place as the coal is always banked against the flight. The amount of coal desired in the major sample is governed by the number of openings of the gate per revolution of the conveyor, and this in turn by the number of arms A that are fastened to the flights. Detection of Carbon Monoxide in Air. L. O. Meyer (Arc/iw fur Hygiene), in a paper on the production of carbon monoxide by various stoves, gives the following particulars of the different methods for estimating the quantity of carbon monoxide present in air (1) Vogel’s, diluted blood solution + reducing agents gives absorption bands in the spectrum; sensitive to 0*25 per cent, of CO. (2) Welzel’s, comparison of colours of precipitates formed in dilute blood solution, treated with pure air or with air to be tested, by tannin; sensitive to 0*0025 per cent, of CO. (3) Winkler’s, absorption of CO by Cu2Cl2 dissolved in an almost saturated solution of NaCl, dilution and addition of palladium chloride (a black cloudy precipitate being formed if CO be present); sensitive to 0*03 per cent, in three hours. (4) Palladium chloride or sodio-palladium chloride paper (preferably damped with sodium acetate solution); sensitive to 0*0005 per cent, of CO in 48 hours, or in 12 hours if the paper be dipped in a 2 per- cent. solution of PdCl4. Method (1) is affected by the presence of other products of combustion, so that CO cannot be found in the chimney gases of a coal fire. Meyer used for his researches the method of Kinnicutt and Sandford, based upon the reaction I2O5 + 5CO = I., + 5CO2; the iodine is dissolved in KI solution, the CO absorbed, and the remaining iodine titrated back by sodium thiosulphate. The air to be tested is, as a pre- liminary, passed through caustic potash, and through sulphuric acid. This method is sensitive to 0*003 per cent, of CO. The Miner’s Acetylene Lamp. Advantages and disadvantages of acetylene lamps for use in coal mines are pointed out by James W. Paul in a recent circular issued by the United States Bureau of Mines. Mr. Paul says : Within recent years there has come into use in metal mines and in many coal mines in the United States a type of open-flame cap lamp for burning acetylene gas, the gas being made within the lamp by the use of calcium carbide and water. In some non-gaseous coal mines this type of lamp has almost entirely taken the place of the miners’ open-flame oil lamp, and in many metal mines it has replaced candles. The number of acetylene lamps in daily use in the AND TECHNOLOGY. mines of the United States is estimated at fully 300,000; 60 per cent, of the lamps used in non-gaseous mines and 15 to 20 per cent, of those in metal mines being acetylene lamps. Some of the advantages that may justly be claimed for carbide lamps are as follow :—‘ ‘ As compared with an ordinary miner’s oil lamp or a candle, a carbide lamp gives much more light. A carbide lamp is clean, and the flame produces little smoke. The gases of combus- tion are principally .carbon dioxide and steam (water vapour), and the acetylene is not injurious to health. The flame will not drop sparks and thus ignite explosives or anything that will burn, as sparks from an oil lamp may do; however, the flame of acetylene will set fire to anything inflammable more quickly than will the flame of an oil lamp or candle. With the better light the working place can be more easily examined, and danger- ous roof conditions can be more readily detected. The general efficiency of the men is increased, because they are able to do more work with a better light. The cost of upkeep of carbide lamps is less than that of oil lamps or candles.” Some of the disadvantages in the use of carbide lamps are as follow :—“ The flame, compared with that of an oil-burning lamp, is more easily put out by a sudden jar or by a shock to the mine air such as is frequently produced by blasting; however, the lamp may be quickly relighted if it is provided with some form of cerium igniter. When the flame is put out before the supply of carbide and water is used, the acetylene produced has a bad smell. As a carbide lamp will burn in air contain- ing less oxygen and more carbon dioxide or blackdamp than will an oil lamp or candle, a miner using a carbide lamp may, without realising it, work in air that is bad for his health or even dangerous to his life. The use of carbide lamps tends to lessen attention to the ventila- tion of the mine, especially as regards the presence of carbon dioxide or blackdamp. Careless or improper handling of carbide, such as permitting a quantity of it to come in contact with a pool of water in a mine, may cause an explosion or burn the men. Carrying carbide in the mine in a glass jar resulted seriously to a miner who accidentally dropped the jar in a wet place and ignited the gas. Cap lamps which have the gas generator attached to the belt of the miner are liable to leak at the generator or its tube connection, and the escaping acetylene gas may take fire and fatally burn the miner. Owing to the ease with which the flame may be put out by sudden jars or by a shock to the air, the carbide lamp is not so well adapted for use by drivers, trip riders, or motormen.” Standardisation of Bomb Calorimeters. The United States Bureau of Standards of the Depart- ment of Commerce has issued a paper describing briefly the methods of calibrating and using bomb calorimeters, such as are used in determining the amount of heat available from a given weight of coal or coke, or other combustible. Provision is made by the Bureau for (standardising these calorimeters by means of standard samples of certain pure materials, viz., sugar, naph- thalene, and benzoic acid. By burning known amounts of these substances in the bomb the observer determines the amount of heat required to raise the temperature of the bomb, together, with the proper amount of water, one degree. The amount of heat furnished by a given sample of coal burned in the same bomb with the same amount of water can then be found. These standard samples serve as standards of heat, and make it possible to get the same results from tests made anywhere. UnexpLoded Dynamite Charges Safely Removed by Air. By inserting the end of a hose or short length of pipe in a blast hole that has failed to go off, turning on a light pressure of air through a valve from the drill line, and withdrawing the pipe with the pressure on, the unexploded dynamite may be removed with safety. The work should be done with care, and too much air pressure should not be turned on. This method was advocated by J. S. Langthorn (in a paper read at a recent meeting of the Brooklyn Engineers’ Club), in preference to attempting to drill a new hole alongside the unexploded one. The paper, which outlined the effective methods used in handling explosives on the Catskill Aqueduct tunnels, and the discussion which followed, dealt with tunnel practice, where the holes in the heading are all drilled at an angle. No one can be sure where the end of such a hole, 8 or 10 ft. from the face, is located, and when one of them has missed, it is dangerous to drill another hole anywhere near it. That this practice is much more dangerous than withdrawing the unexploded charge with care, especially where com- pressed air is used, was unanimously asserted by several tunnel engineers of wide reputation, who took part in the discussion of the paper. J. R. Healy, inspector of com- bustibles of the Bureau of Fire Prevention, stated that where compressed air was used as described, the charge followed the pipe out of the hole as though it were a piece of iron and the pipe a powerful magnet. THE GERMAN AND AUSTRIAN COAL AND IRON TRADES. We give below further extracts from German periodicals that have reached us, showing the course of the coal and iron trades in Germany and Austria :— The Rhenish Westphalian Iron Market. There is little change in the conditions which determine the situation, the restriction of output (through scarcity of labour) and the increased cost of production still prevailing. On the other hand, prices of finished products have • fallen to some extent, apparently because the trade hopes to recover its require- ments at a lower figure later on. Against this, the works are holding out because of the manifest tendency of raw materials to keep on the up grade. The ore market continues firm, but supplies are increasing, the Siegerland mines having succeeded in considerably improving their output, the whole of which is disposed of with ease. The scarcity of railway trucks, however, has hindered deliveries and necessitated stock- ing at the mines, thus increasing the expenses. Prices remaiin unaltered at 15*60 mk. for raw spathic ore, 24*50 mk. for roasted, and 16*50 mk. for brown ironstone. No rates have yet been fixed for next quarter’s sales, but an advance is expected. Nassau red ironstone is quiet at about 20-21 mk. A prominent feature of the situation is that slags from Siegerland blast furnaces are being largely shipped to iron works in South-West Germany. They contain about 8-10 per cent, of manganese, and are sold at 3-4 mk. per ton for mixing with Lothningen ores. Minette (30 per cent.) fetches about 3 mk. per ton, richer ores correspondingly higher prices, Fernie ore being quoted at 21-25 mk. Pig iron of good quality is in active demand, and the output increasing, but phosphoritic brands are in less request. Prices remain as before, but are expected to advance for the coming quarter, as a consequence of the anticipated advance in raw materials. Scrap is particu- larly abundant, and prices are therefore weak, without prospect of any immediate improvement. Heavy casting scrap, which some months ago was fetching 85-90 mk., has receded to about 65-66mk., railway shop turnings are 45-46 mk., prime core scrap 54-56 mk., fresh heavy waste 57-59 mk., and casting turnings 45-46 mk. The trade in semis continues on the same fines as before, the demand for plate bars being specially active. Ordinary blooms sell at about 120 mk. and high grade at 130 mk., free works. In bars, whilst the Convention has not yet been formally abrogated, it is practically non-existent; one large works, in want of orders, having offered at 125 mk., as compared with the Convention price of 140 mk. The tenders put forward recently at Cologne were'still lower, but whether the merchants in question were actually backed by any of the works has not transpired. The large Rhenish-Westphalian mills are adhering to the Convention rates, and up to 145 mk. are obtained for small parcels to particular specifications. Universal iron, after falling to 135 mk., has recovered. As a rule, the works are well booked with orders, some up to and beyond the end of next February. Welding iron is quoted at 163 mk., horse-shoe bars at 182 mk., chain and rivet bars at 195 mk. ex works. Girders are still quiet, at 130 mk. ex Diedenhofen; but of late, large orders have been placed for structural iron and wagon builders’ materials. The heavy plate market has shown a weakening tendency in harmony with the fluctuations in bar prices, and offers have been made below the Convention price of 140 mk. The works are, however, well booked for forward delivery (some up to the end of April), and are little disposed to give way in the matter of price. Export rates are higher than those in the home market, ship plate, for instance, having been sold recently at 205 mk. ex works, as compared with the home price of 150 mk. for heavy plate, and 155 mk. for special qualities. Structural plate costs 157-50 mk., No. 1 boiler plate 165 mk. Medium plate has gone back a little, to about 155 mk. ex works, but fine plate remains at 180 to 185 mk., thinner sorts fetching about 190 mk. In the wire market, rolled wire is unusually cheap, as a result of the lowered rates for bars, although the Con- vention prices are still in force. Mild open hearth steel wire costs 155 mk., drawn wire 180 mk., nail wire 177*50 mk., screw and rivet wire 257 m., galvanised wire 225 mk., barbed wire (No. 28) 285 m., nails 190 mk. Business in railway superstructural material is quiet, but even then the works cannot keep up with the demand. There is little doing in pit and field railway rails, but prices remain unchanged. The German Bar Iron Market. The bar iron merchants in the Dortmund district met on the 11th inst. to discuss the question of how far the situation created by the lowered tenders for railway material at Cologne will affect prices of stock goods. It was generally considered that the Essen merchants who had tendered at 10 to 12 mk. below all other com- peting firms, were not covered by contracts with manu- facturers. It was also stated that the mills are well booked with orders, and unlikely to accept business, for large quantities, below existing Convention prices. In view of the increasing tendency of costs of production, the meeting decided not to make any change for the present in the prices of stock goods.